Methoxyacetone → HCID 13051537、化合物

HRID 462582

反応式

HRID 462582 の反応式
[C:1]([C:4]1[C:9]([OH:10])=[C:8]([CH3:11])[C:7]([CH3:12])=[C:6]([OH:13])[C:5]=1[CH3:14])(=[O:3])[CH3:2].[CH3:15][O:16][CH2:17][C:18](=O)[CH3:19].N1CCCC1>C1(C)C=CC=CC=1>[OH:13][C:6]1[C:5]([CH3:14])=[C:4]2[C:9](=[C:8]([CH3:11])[C:7]=1[CH3:12])[O:10][C:18]([CH2:17][O:16][CH3:15])([CH3:19])[CH2:2][C:1]2=[O:3]

参加物

5

反応物 3

HCID 22172MethoxyacetoneHCID 31268PyrrolidineHCID 10867205Ethanone, 1-(2,5-dihydroxy-3,4,6-trimethylphenyl)-

生成物 1

HCID 13051537HCID 13051537、化合物収率 37%

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

3.00 g (15.6 mmoles) of acetyl-trimethylhydroquinone, 1.58 g (18 mmoles) of methoxyacetone and 250 g (30 mmoles) of pyrrolidine were reacted in toluene solution by a method similar to that of Example 1 to give the above product, which was obtained as an oil. Boiling point: 250°-270° C. (bulb tube); yield: 37%.

後処理

  1. customto give the above product
  2. customwhich was obtained as an oil

出典と根拠

ORDレコード
ord-b11016a754104f75b76edaf66f801acf
出典データセット
uspto-grants-1985_05
特許番号
US04515975

関連ノート

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