Thionyl Chloride → HCID 178444542、化合物

HRID 462875

反応式

HRID 462875 の反応式
[CH2:1]([C@H:6]1[CH2:11][CH2:10][C@H:9]([C:12]([OH:14])=O)[CH2:8][CH2:7]1)[CH2:2][CH2:3][CH2:4][CH3:5].S(Cl)([Cl:17])=O>>[CH2:1]([C@H:6]1[CH2:11][CH2:10][C@H:9]([C:12]([Cl:17])=[O:14])[CH2:8][CH2:7]1)[CH2:2][CH2:3][CH2:4][CH3:5]

参加物

3

反応物 2

HCID 24386Thionyl ChlorideHCID 178444557HCID 178444557、化合物

生成物 1

HCID 178444542HCID 178444542、化合物

実験手順

5.58 g Of trans-4-pentylcyclohexylcarboxylic acid was heated with 20 ml of thionyl chloride under reflux conditions. After the reaction was completed, the excess of thionyl chloride was removed completely under reduced pressure and the product residue obtained was distilled under reduced pressure. Trans-4-pentylcyclohexylcarbonyl chloride having a boiling point of 103° to 105° C./0.5 mmHg was obtained.

後処理

  1. customthe excess of thionyl chloride was removed completely under reduced pressure
  2. customthe product residue obtained
  3. distillationwas distilled under reduced pressure

出典と根拠

ORDレコード
ord-a6066b6dbaaa4fe79ddd37f85dbd565e
出典データセット
uspto-grants-1985_05
特許番号
US04518226

関連ノート

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