Methyl iodide → Methyl 4-chlorobenzene-1-carboximidothioate hydroiodide

HRID 463883ノート

反応式

HRID 463883 の反応式
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH2:8])=[S:7])=[CH:4][CH:3]=1.[CH3:11][I:12]>CC(C)=O>[IH:12].[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([S:7][CH3:11])=[NH:8])=[CH:4][CH:3]=1

参加物

4

反応物 2

HCID 6328Methyl iodideHCID 27348264-Chlorothiobenzamide

生成物 1

HCID 2777317Methyl 4-chlorobenzene-1-carboximidothioate hydroiodide

試薬・触媒・溶媒 1

HCID 180Acetone溶媒

実験手順

A 17.16 g portion of 4-chlorothiobenzamide was dissolved in 80 ml of acetone and 15.14 g of methyl iodide was added. The mixture was stirred for 2 hours and then the solid was collected, washed with acetone and dried, giving 21.3 g of 4-chlorobenzenecarboximidothioic acid, methyl ester, hydroiodide.

後処理

  1. customthe solid was collected
  2. washwashed with acetone
  3. customdried

出典と根拠

ORDレコード
ord-1ede6d8960aa44a1ae0763510bf475ee
出典データセット
uspto-grants-1985_10
特許番号
US04544759

反応ノート

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