4-(Octyloxy)benzoic acid → 4-Octyloxy-3-bromobenzoic acid
反応式
[CH2:1]([O:9][C:10]1[CH:18]=[CH:17][C:13]([C:14]([OH:16])=[O:15])=[CH:12][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[Br:19]Br>O>[CH2:1]([O:9][C:10]1[CH:11]=[CH:12][C:13]([C:14]([OH:16])=[O:15])=[CH:17][C:18]=1[Br:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]参加物
4
実験手順
A 25 g (0.1 mole) amount of p-octyloxybenzoic acid was suspended in 120 ml of water. The temperature was increased to between 50° C. and 55° C. and 17.6 g (0.11 mole) of bromine were added over a period of 7 hours at that temperature. The suspended solids were then filtered and recrystallized from ethanol and pure 4-octyloxy-3-bromobenzoic acid was obtained.
後処理
- temperatureThe temperature was increased to between 50° C. and 55° C.
- filtrationThe suspended solids were then filtered
- customrecrystallized from ethanol
出典と根拠
- ORDレコード
- ord-a3cd020d4ab04b65b1bc5990ffdfda26
- 出典データセット
- uspto-grants-1979_11
- 特許番号
- US04173545
反応ノート
読み込み中…