化工社化工社 化学情報印刷レポート · 研究参考用
Methanol → 3-Phenyl-1-indanone oxime
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 1-Indanone, 3-phenyl- | HCID 98146 | — |
| 反応物 | Hydroxyamine hydrochloride | HCID 443297 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 3-Phenyl-1-indanone oxime | HCID 73183939 | — |
反応手順
A mixture of 3-phenylindan-1-one (80 g), methanol (935 ml), water (90 ml), potassium carbonate (103.8 g), and hydroxylamine HCl (104.3 g) was heated at reflux for 16 hours, then poured into ice-water: the title compound was filtered, washed with water, with a small portion of ether, then dried in air. Yield: 74.7 g; m.p. 133°-139°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04548946 |
| 出典データセット | uspto-grants-1985_10 |
| ORD ID | ord-06804961a4a94f6fab538831a07fec43 |
| 出典メモ | uspto-grants-1985_10 |