Trifop → HCID 13505617、化合物

HRID 464912

反応式

HRID 464912 の反応式
[F:1][C:2]([F:23])([F:22])[C:3]1[CH:21]=[CH:20][C:6]([O:7][C:8]2[CH:19]=[CH:18][C:11]([O:12][CH:13]([CH3:17])[C:14](O)=[O:15])=[CH:10][CH:9]=2)=[CH:5][CH:4]=1.[Cl:24][C:25]1[CH:30]=[CH:29][C:28]([Cl:31])=[CH:27][C:26]=1[S:32]([N:35]=C=O)(=[O:34])=[O:33]>>[Cl:24][C:25]1[CH:30]=[CH:29][C:28]([Cl:31])=[CH:27][C:26]=1[S:32]([NH:35][C:14](=[O:15])[CH:13]([O:12][C:11]1[CH:10]=[CH:9][C:8]([O:7][C:6]2[CH:20]=[CH:21][C:3]([C:2]([F:23])([F:1])[F:22])=[CH:4][CH:5]=2)=[CH:19][CH:18]=1)[CH3:17])(=[O:33])=[O:34]

参加物

3

反応物 2

HCID 181206TrifopHCID 128751872,5-Dichlorobenzene-1-sulfonyl isocyanate

生成物 1

HCID 13505617HCID 13505617、化合物

実験手順

A solution of one gram (0.0031 mole) 2-[4-(4-trifluoromethylphenoxy)phenoxy]-propionic acid in dry CHCH3 was treated with 0.8 gram (g) (0.0081 mole) 2,5-dichlorobenzene sulfonyl isocyanate. The solution was stirred for approximately 18 hours, then heated to reflux for three hours, followed by cooling.

後処理

  1. temperatureheated
  2. temperatureto reflux for three hours
  3. temperatureby cooling

出典と根拠

ORDレコード
ord-1964ed97a263462cb25e4e9a6d4bd11f
出典データセット
uspto-grants-1985_10
特許番号
US04549901

関連ノート

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