Hydrochloric Acid → HCID 178421680、化合物

HRID 46798

反応式

HRID 46798 の反応式
C(N[C:6](=[O:13])[C:7]([C:9]1([CH3:12])[CH2:11][CH2:10]1)=O)(C)(C)C.[NH2:14][NH:15][C:16]([NH:18][NH2:19])=[S:17].Cl.C(O)C>O>[NH2:14][N:15]1[C:6](=[O:13])[C:7]([C:9]2([CH3:12])[CH2:11][CH2:10]2)=[N:19][N:18]=[C:16]1[SH:17]

参加物

6

反応物 4

HCID 313Hydrochloric AcidHCID 702EthanolHCID 2724189ThiocarbohydrazideHCID 20385839(1-Methylcyclopropyl)-glyoxylic acid tert-butylamide

生成物 1

HCID 178421680HCID 178421680、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

183 grams of (1-methyl-cyclopropyl)-glyoxalic acid-tert.-butylamide and 112 grams of thiocarbohydrazide were added to a mixture of 1 liter of 1 normal HCl and 1 liter of ethanol. The mixture was boiled under reflux for 8 hours, cooled, diluted with 2 liters of water and the crystals filtered off with suction. There were obtained white crystals with a yellow luster which were dried.

後処理

  1. temperatureunder reflux for 8 hours
  2. temperaturecooled
  3. filtrationthe crystals filtered off with suction
  4. customThere were obtained white crystals with a yellow luster which
  5. customwere dried

出典と根拠

ORDレコード
ord-e471648b4ae44be4b25f0eae45b4618f
出典データセット
uspto-grants-1979_11
特許番号
US04175188

関連ノート

読み込み中…