化工社化工社 化学情報印刷レポート · 研究参考用
1,6-Diiodohexane → 1,1'-Hexane-1,6-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione}
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,6-Diiodohexane | HCID 12373 | — |
| 反応物 | 1,1'-Butane-1,4-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione} | HCID 49763837 | — |
| 生成物 | 1,1'-Hexane-1,6-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione} | HCID 49763838 | 27% |
反応手順
The experimental protocol used is the same as that described for the synthesis of the compound of Example 1, 1,6-diiodohexane replacing 1,4-dibromobutane. The expected compound is obtained in the form of a light yellow solid with a yield of 27%. Melting point: 187-188° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08624037B2 |
| 出典データセット | uspto-grants-2014_01 |
| ORD ID | ord-3ea8d0c5a6b24f7daeb679b1c6c2cb68 |
| 出典メモ | uspto-grants-2014_01 |