化工社化工社 化学情報印刷レポート · 研究参考用
4-Methyl-3-oxopentanal → 2-Benzylthio-2-benzylthio-5-isopropyl-1,2,4-triazolo[1,5-a]pyrimidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methyl-3-oxopentanal | HCID 14786268 | — |
| 反応物 | HCID 178509291 | HCID 178509291 | — |
| 生成物 | 2-Benzylthio-2-benzylthio-5-isopropyl-1,2,4-triazolo[1,5-a]pyrimidine | HCID 19837373 | 96% |
反応手順
This material was prepared in 96% yield from 3-amino-5-benzylthio-1,2,4-triazole and 4-methyl-3-oxopentanal following the general procedure described in Example 7. The desired product was isolated as a solid, m.p. 65°-66° C. IR and 1H NMR were in agreement with the assigned structure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04886883 |
| 出典データセット | uspto-grants-1989_12 |
| ORD ID | ord-22ff46e77d9043b5808adaebdf58274d |
| 出典メモ | uspto-grants-1989_12 |