Dimethyl Disulfide → 2-Fluoro-6-(methylsulfanyl)aniline
反応式
C(OC([NH:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[F:15])=O)(C)(C)C.[CH3:16][S:17]SC>>[F:15][C:10]1[CH:11]=[CH:12][CH:13]=[C:14]([S:17][CH3:16])[C:9]=1[NH2:8]参加物
3
実験手順
This material was prepared for N-t-butoxycarbonyl-2-fluoroaniline and dimethyl disulfide following the general procedure outlined in Example 102. IR and 1H NMR spectra of the product were consistent with the assigned structure.
出典と根拠
- ORDレコード
- ord-98ae86c9e0ee48de98980381426fc8d8
- 出典データセット
- uspto-grants-1989_12
- 特許番号
- US04886883
反応ノート
読み込み中…