2-Nitrophenol → HCID 15017530、化合物

HRID 477268

反応式

HRID 477268 の反応式
[Cl:1][C:2]1[C:3](F)=[N:4][CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.[N+:13]([C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1[OH:22])([O-:15])=[O:14]>>[Cl:1][C:2]1[C:3]([O:22][C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][C:16]=2[N+:13]([O-:15])=[O:14])=[N:4][CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1

参加物

3

反応物 2

HCID 69472-NitrophenolHCID 12680753-Chloro-2-fluoro-5-(trifluoromethyl)pyridine

生成物 1

HCID 15017530HCID 15017530、化合物収率 63%

実験手順

This material was prepared in 63% yield from 3-chloro-2-fluoro-5-trifluoromethylpyridine and 2-nitrophenol following the general procedure outlined in Example 104. The product was isolated as an amber oil which was characterized by IR and 1H NMR spectroscopy.

後処理

  1. customThe product was isolated as an amber oil which

出典と根拠

ORDレコード
ord-ee74605885a04bcebaa429762abca957
出典データセット
uspto-grants-1989_12
特許番号
US04886883

関連ノート

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