Potassium Hydroxide → Potassium cinnamate

HRID 479263ノート

反応式

HRID 479263 の反応式
[CH:1]1[CH:2]=[CH:3][C:4](/[CH:7]=[CH:8]/[CH2:9][OH:10])=[CH:5][CH:6]=1.[OH-:11].[K+:12]>C1(C)C=CC=CC=1>[C:9]([O-:11])(=[O:10])[CH:8]=[CH:7][C:4]1[CH:5]=[CH:6][CH:1]=[CH:2][CH:3]=1.[K+:12]

参加物

4

反応物 2

HCID 14797Potassium HydroxideHCID 5315892Cinnamyl Alcohol

生成物 1

HCID 44135689Potassium cinnamate

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

50 g (0,36 mol) of cinnamic alcohol are dissolved in 180 ml of dry toluene. 20 g (0,36 mol) of KOH are added to the solution, and the resulting mixture is kept under stirring for one hour at room temperature. During this phase, potassium cinnamate is obtained. Then, a solution prepared starting from 18 g (0,10 mol) of 2,4,6-trichloro-s-triazine in 150 ml of toluene is added, allowing to react at room temperature for further 90 hours under stirring.

出典と根拠

ORDレコード
ord-4f889249f22e44c297275e8a0c6e5abd
出典データセット
uspto-grants-2003_11
特許番号
US06645396B2

反応ノート

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