Thionyl Chloride → 2-(Octyloxy)benzoyl chloride
反応式
[CH2:1]([O:9][C:10]1[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=1[C:12](O)=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(Cl)([Cl:21])=O>>[CH2:1]([O:9][C:10]1[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=1[C:12]([Cl:21])=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]参加物
3
実験手順
First, octyloxybenzoic acid was heated in thionyl chloride under reflux until complete dissolution. Excess thionyl chloride was removed by vacuum distillation. Thus there was obtained octyloxybenzoic acid chloride.
後処理
- temperatureunder reflux until complete dissolution
- customExcess thionyl chloride was removed by vacuum distillation
出典と根拠
- ORDレコード
- ord-65b436956dee4667b9a4e64adcfcd867
- 出典データセット
- uspto-grants-1993_07
- 特許番号
- US05225105
反応ノート
読み込み中…