Dimethylamine → 1-[4-(Dimethylamino)-2-butynyl]-2-imidazolidinone

反応式

C[N:2]1[CH2:6][CH2:5][N:4]([CH2:7][C:8]#[CH:9])[C:3]1=[O:10].[CH3:11][NH:12][CH3:13].N1CCC[CH2:15]1>>[CH3:11][N:12]([CH3:15])[CH2:13][C:9]#[C:8][CH2:7][N:4]1[CH2:5][CH2:6][NH:2][C:3]1=[O:10]

参加物

反応物 3

HCID 674Dimethylamine

HCID 31268Pyrrolidine

HCID 113555131-Methyl-3-(2-propynyl)-2-imidazolidinone

生成物 1

HCID 150655151-[4-(Dimethylamino)-2-butynyl]-2-imidazolidinone

実験手順

This product was prepared according to Example 1, Part B, by substituting 1-(2-propynyl)-2-imidazolidinone for 1-methyl-3-(2-propynyl)-2-imidazolidinone and dimethylamine for pyrrolidine; m.p. 83°-87° C.

後処理

customThis product was prepared

出典と根拠

ORDレコード: ord-beeeac4f52414081ad07026a2fd9c553
出典データセット: uspto-grants-1993_07
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05225567

反応ノート

読み込み中…