Aluminum nitrate nonahydrate → Dialuminium cobalt tetraoxide

HRID 483763

反応式

HRID 483763 の反応式
O.O.O.O.O.O.[N+]([O-])([O-])=[O:8].[Co+2:11].[N+]([O-])([O-])=[O:13].O.O.O.O.O.O.O.O.O.[N+]([O-])([O-])=[O:26].[Al+3:29].[N+]([O-])([O-])=[O:31].[N+]([O-])([O-])=[O:35].C(=O)([O-])[O-].[NH4+].[NH4+]>O>[O-2:8].[O-2:13].[O-2:26].[O-2:31].[O-2:35].[Al+3:29].[Al+3:29].[Co+2:11].[Co+2:11]

参加物

5

反応物 3

HCID 24567Aluminum nitrate nonahydrateHCID 24821Cobaltous nitrate hexahydrateHCID 517111Ammonium Carbonate

生成物 1

HCID 159384Dialuminium cobalt tetraoxide

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

In 300 ml of pure water were dissolved 29 g of cobalt nitrate hexahydrate and 75 g of aluminum nitrate nonahydrate. A solution of 38.4 g of ammonium carbonate dissolved in 100 ml of pure water was gradually added thereto with stirring to form a gel-form precipitate. The precipitate was washed with pure water three times, dried at 100° C. overnight and calcined at 600° C. in an air stream. The calcined material was then calcined at 800° C. in a muffle furnace for 3 hours to a cobalt aluminate catalyst having a blue color.

後処理

  1. additionwas gradually added
  2. customto form a gel-form precipitate
  3. washThe precipitate was washed with pure water three times
  4. customdried at 100° C. overnight
  5. customcalcined at 600° C. in an air stream

出典と根拠

ORDレコード
ord-d755ad4082d34d449f7b2c97f1c17329
出典データセット
uspto-grants-1993_07
特許番号
US05227145

関連ノート

読み込み中…