2,6-Dimethyl-4-nitroaniline → 2-[(2,6-Dimethyl-4-nitrophenyl)amino]-1-pyrroline

HRID 484787

反応式

HRID 484787 の反応式
Cl[C:2]1[CH2:6][CH2:5][CH2:4][N:3]=1.[CH3:7][C:8]1[CH:14]=[C:13]([N+:15]([O-:17])=[O:16])[CH:12]=[C:11]([CH3:18])[C:9]=1[NH2:10]>>[CH3:7][C:8]1[CH:14]=[C:13]([N+:15]([O-:17])=[O:16])[CH:12]=[C:11]([CH3:18])[C:9]=1[NH:10][C:2]1[CH2:6][CH2:5][CH2:4][N:3]=1

参加物

3

反応物 2

HCID 281592,6-Dimethyl-4-nitroanilineHCID 135201412-Chloro-1-pyrroline

生成物 1

HCID 202723942-[(2,6-Dimethyl-4-nitrophenyl)amino]-1-pyrroline

実験手順

A mixture of 2-chloro-1-pyrroline, prepared as in Example 1, and 19.9 g (0.12 mole) of the aniline product of Example 6 were heated at reflux overnight, according to the general method of Example 8. The title compound was isolated and used for subsequent reactions without further purification. Structure assignment was supported by nmr and infrared spectra.

後処理

  1. temperaturewere heated
  2. temperatureat reflux overnight

出典と根拠

ORDレコード
ord-b73808b27f264206b52ae5c5d7b1945f
出典データセット
uspto-grants-1985_08
特許番号
US04533739

関連ノート

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