Sulfuric Acid → HCID 86740245、化合物

HRID 485078ノート

反応式

HRID 485078 の反応式
[C:1](#[N:4])[CH:2]=[CH2:3].[CH3:5][O:6][C:7](=[O:14])[C:8]([S:10]([OH:13])(=[O:12])=[O:11])=[CH2:9].S(=O)(=O)(O)O>O>[C:1](#[N:4])[CH:2]=[CH2:3].[CH3:5][O:6][C:7](=[O:14])[C:8]([S:10]([OH:13])(=[O:12])=[O:11])=[CH2:9]

参加物

5

反応物 3

HCID 1118Sulfuric AcidHCID 7855AcrylonitrileHCID 212196153-Methoxy-3-oxoprop-1-ene-2-sulfonic acid

生成物 1

HCID 86740245HCID 86740245、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

200 ml of distilled water, 15 g of monomer made up of 99 to 80% by weight of acrylonitrile and 1 to 20% by weight of 2-sulphopropenoic acid methyl ester and 0.5 g of 1-N sulphuric acid were introduced into a reaction vessel. After nitrogen had been passed through and the polymerization mixture tempered at 55° C., polymerization was initiated by the addition of 15 ml of each of the following solutions I and II.

後処理

  1. additionwere introduced into a reaction vessel
  2. customtempered at 55° C.
  3. custompolymerization

出典と根拠

ORDレコード
ord-3345eb442d324b7db6005b3af53f0978
出典データセット
uspto-grants-1985_08
特許番号
US04535139

反応ノート

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