Azobisisobutyronitrile → HCID 86740248、化合物

反応式

[C:1]([O:4][CH:5]=[CH2:6])(=[O:3])[CH3:2].[CH3:7][O:8][C:9](=[O:17])[C:10]([S:12]([O:15][CH3:16])(=[O:14])=[O:13])=[CH2:11].N(C(C)(C)C#N)=NC(C)(C)C#N>>[C:1]([O:4][CH:5]=[CH2:6])(=[O:3])[CH3:2].[CH3:7][O:8][C:9](=[O:17])[C:10]([S:12]([O:15][CH3:16])(=[O:14])=[O:13])=[CH2:11]

参加物

反応物 3

HCID 6547Azobisisobutyronitrile

HCID 7904Vinyl Acetate

HCID 54531152Methyl 2-(methoxysulfonyl)prop-2-enoate

生成物 1

HCID 86740248HCID 86740248、化合物

実験手順

After tempering at 65° C. and an increase in the viscosity of the mixture, a solution of 80 g of vinyl acetate, 20 g of 2-methoxysulphonyl propenoic acid methyl ester (11 mole percent) and 0.4 g of 2,2'-azo-bis-isobutyronitrile was added over a period of 1 hour.