Pyridine → 1-(2-Methoxy-2-oxoethyl)pyridinium chloride
反応式
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl:7][CH2:8][C:9]([O:11][CH3:12])=[O:10]>C(OCC)(=O)C>[Cl-:7].[CH3:12][O:11][C:9]([CH2:8][N+:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)=[O:10]参加物
4
実験手順
Pyridine (1 equivalent) and methyl chloroacetate (1 equivalent) in ethyl acetate were heated (80° C.) for 24 hours. The reaction mixture was cooled to room temperature and the resulting crystalline pyridinium salt filtered, washed with ethyl acetate, and dried in vacuum.
後処理
- filtrationthe resulting crystalline pyridinium salt filtered
- washwashed with ethyl acetate
- customdried in vacuum
出典と根拠
- ORDレコード
- ord-d6f60419ed23424aa2a11487ac3fbb00
- 出典データセット
- uspto-grants-1994_03
- 特許番号
- US05294721
反応ノート
読み込み中…