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2,3,4-Trichloronitrobenzene → 4-Carbobenzyloxy-1-(5,6-dichloro-2-nitrophenyl)piperazine-2-carboxylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3,4-Trichloronitrobenzene | HCID 28697 | — |
| 反応物 | 4-((Benzyloxy)carbonyl)piperazine-2-carboxylic acid | HCID 5058362 | — |
| 生成物 | 4-Carbobenzyloxy-1-(5,6-dichloro-2-nitrophenyl)piperazine-2-carboxylic acid | HCID 21976687 | 43.6% |
反応手順
By the same procedure described for Example 7 A, from 0.86 g of 2,3,4-trichloro-nitro-benzene and 1.0 g of 4-carbobenzyloxypiperazine-2-carboxylic acid, there was obtained 0.75 g of the desired product as a brown oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06706714B2 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-fabb7311f562439b82a73e4d38dda136 |
| 出典メモ | uspto-grants-2004_03 |