関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Azobisisobutyronitrile | HCID 6547 | — |
| 反応物 | Acrolein | HCID 7847 | — |
| 反応物 | Propylene glycol methyl ether acetate | HCID 7946 | — |
| 反応物 | 4-Bromostyrene | HCID 16263 | — |
| 反応物 | Methacrylate | HCID 87595 | — |
| 生成物 | Bromostyrene acrolein methacrylate | HCID 86612195 | — |
反応手順
3 g of 4-bromostyrene, 4 g of acrolein, 3 g of methacrylate and 0.2 g of AIBN were sufficiently mixed with 50 g of PGMEA. The mixture was polymerized by heating the mixture at 67° C. for 8 hours. After completion of the polymerization, the polymerization product was precipitated in n-hexane, filtered, and dried in vacuo to give a poly(bromostyrene-acrolein-methacrylate) copolymer.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07531297B2 |
|---|
| 出典データセット | uspto-grants-2009_05 |
|---|
| ORD ID | ord-56c73c674f6e45feb107ca90d3d30919 |
|---|
| 出典メモ | uspto-grants-2009_05 |
|---|
