Phenylphosphonic Acid → HCID 21506410、化合物

HRID 492039

反応式

HRID 492039 の反応式
[C:1]1([P:7](=[O:10])([OH:9])[OH:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH-].[Mg+2:12].[OH-]>O>[C:1]1([P:7](=[O:8])([O-:10])[O-:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Mg+2:12]

参加物

4

反応物 2

HCID 15295Phenylphosphonic AcidHCID 73981Magnesium Hydroxide

生成物 1

HCID 21506410HCID 21506410、化合物収率 99%

試薬・触媒・溶媒 1

HCID 962Water溶媒

反応条件

温度
80 °C

実験手順

1.58 g (10.0 mmol) of phenylphosphonic acid (manufactured by Nissan Chemical industries, Ltd.), 0.583 g (10.0 mmol) of magnesium hydroxide and 41 g of water were mixed, stirred at 80° C. for 3 hours, then water was distilled off under reduced pressure and dried at 200° C. to obtain 1.78 g (yield 99%) of the aimed product as white crystal. Decomposition temperature: 524° C.

後処理

  1. distillationwater was distilled off under reduced pressure
  2. customdried at 200° C.

出典と根拠

ORDレコード
ord-c57a87bc93e14e7fbbb1c2c9a1a8f65f
出典データセット
uspto-grants-2009_05
特許番号
US07531585B2

関連ノート

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