化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → Ethyl 4'-hydroxy-4-biphenylcarboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | 4-Propylbenzoic acid | HCID 137601 | — |
| 反応物 | 4'-Hydroxy-4-biphenylcarboxylic acid | HCID 301556 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Ethyl 4'-hydroxy-4-biphenylcarboxylate | HCID 4049156 | — |
反応手順
The reaction was conducted in the same manner as in the step (i) of the Example 33, except for using 4-(4-hydroxyphenyl)benzoic acid and ethanol in lieu of 4-n-propylbenzoic acid and methanol, respectively, and the resultant was recrystallized from toluene to give ethyl 4-(4-hydroxyphenyl)benzoate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07534547B2 |
| 出典データセット | uspto-grants-2009_05 |
| ORD ID | ord-9202b041f1b14830b03a07aa49b22dea |
| 出典メモ | uspto-grants-2009_05 |