化工社化工社 化学情報印刷レポート · 研究参考用
1,1-Dimethylethyl N-(2-amino-4-chlorophenyl)carbamate → HCID 86589303、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,1-Dimethylethyl N-(2-amino-4-chlorophenyl)carbamate | HCID 57456272 | — |
| 反応物 | 3-[3-(2,6-Dimethyl-pyridin-4-yl)-phenyl]-3-oxo-propionic acid tert-butyl ester | HCID 69489240 | — |
| 生成物 | HCID 86589303 | HCID 86589303 | — |
反応手順
The title compound was prepared from (2-amino-4-chloro-phenyl)-carbamic acid tert-butyl ester (Example J4) (243 mg, 1.0 mmol) and 3-[3-(2,6-dimethyl-pyridin-4-yl)-phenyl]-3-oxo-propionic acid tert-butyl ester (Example K15) (325 mg, 1.0 mmol) according to the general procedure M. Obtained as a light brown foam (240 mg, 49%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06949542B2 |
| 出典データセット | uspto-grants-2005_09 |
| ORD ID | ord-2cdeb951fbd1487999477424c3574e10 |
| 出典メモ | uspto-grants-2005_09 |