Ammonia → HCID 178512765、化合物

HRID 49934

反応式

HRID 49934 の反応式
[NH2:1][CH2:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=[O:8])=[CH:5][CH:4]=1.N.[N:13]#[C:14][NH2:15]>O>[NH:1]([CH2:2][C:3]1[CH:4]=[CH:5][C:6]([C:7]([OH:9])=[O:8])=[CH:10][CH:11]=1)[C:14]([NH2:15])=[NH:13]

参加物

5

反応物 3

HCID 222AmmoniaHCID 9864CyanamideHCID 655264-(Aminomethyl)Benzoic Acid

生成物 1

HCID 178512765HCID 178512765、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

反応条件

温度
60 °C

実験手順

A mixture of 1.51 g (10.0 mmol) of 4-aminomethylbenzoic acid, 20 ml of water, 2.0 ml of 28% aqueous ammonia and 1.00 g (23.8 mmol) of cyanamide was stirred at 60° C. overnight. The white precipitate thus formed was taken by the filtration, washed with water and dried to obtain the title compound.

後処理

  1. customThe white precipitate thus formed
  2. filtrationwas taken by the filtration
  3. washwashed with water
  4. customdried

出典と根拠

ORDレコード
ord-c887df8de4df4a55a09c1569fe4de64f
出典データセット
uspto-grants-2004_03
特許番号
US06710056B2

関連ノート

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