Methacrylic anhydride → HCID 86615999、化合物

HRID 499946

反応式

HRID 499946 の反応式
[CH3:1][CH:2]([OH:13])[CH2:3][O:4][CH:5]([CH2:7][O:8][CH:9]([CH2:11][OH:12])[CH3:10])[CH3:6].[C:14]([O:19]C(=O)C(C)=C)(=[O:18])[C:15]([CH3:17])=[CH2:16]>O1CCCC1>[C:14]([OH:19])(=[O:18])[C:15]([CH3:17])=[CH2:16].[CH3:1][CH:2]([OH:13])[CH2:3][O:4][CH:5]([CH2:7][O:8][CH:9]([CH2:11][OH:12])[CH3:10])[CH3:6]

参加物

4

反応物 2

HCID 12974Methacrylic anhydrideHCID 326112-(2-(2-Hydroxypropoxy)propoxy)-1-propanol

生成物 1

HCID 86615999HCID 86615999、化合物

試薬・触媒・溶媒 1

HCID 8028Tetrahydrofuran溶媒

実験手順

In a 0.5 L separable flask, 0.1 mol of tripropylene glycol and 0.1 mol of methacrylic anhydride were mixed in anhydrous tetrahydrofuran. After stirring the mixture for a while, the internal pressure of the container was reduced to volatile the content and the material was distilled off to obtain tripropylene glycol monomethacrylate.

後処理

  1. distillationthe material was distilled off

出典と根拠

ORDレコード
ord-2eaa2d1a4fd143a79701feee30e9cbde
出典データセット
uspto-grants-2010_08
特許番号
US07767753B2

関連ノート

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