Methacrylic anhydride → Tripropylene glycol monomethacrylate
反応式
[CH3:1][CH:2]([OH:13])[CH2:3][O:4][CH:5]([CH2:7][O:8][CH:9]([CH2:11][OH:12])[CH3:10])[CH3:6].[C:14]([O:19]C(=O)C(C)=C)(=[O:18])[C:15]([CH3:17])=[CH2:16]>O1CCCC1>[C:14]([OH:19])(=[O:18])[C:15]([CH3:17])=[CH2:16].[CH3:1][CH:2]([OH:13])[CH2:3][O:4][CH:5]([CH2:7][O:8][CH:9]([CH2:11][OH:12])[CH3:10])[CH3:6]参加物
4
実験手順
In a 0.5 L separable flask, 0.1 mol of tripropylene glycol and 0.1 mol of methacrylic anhydride were mixed in anhydrous tetrahydrofuran. After stirring the mixture for a while, the internal pressure of the container was reduced to volatile the content and the material was distilled off to obtain tripropylene glycol monomethacrylate.
後処理
- distillationthe material was distilled off
出典と根拠
- ORDレコード
- ord-2eaa2d1a4fd143a79701feee30e9cbde
- 出典データセット
- uspto-grants-2010_08
- 特許番号
- US07767753B2
反応ノート
読み込み中…