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Phenol → 4'-Phenoxyacetophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenol | HCID 996 | — |
| 反応物 | Dimethylacetamide | HCID 31374 | — |
| 生成物 | 4'-Phenoxyacetophenone | HCID 236783 | — |
反応手順
4-Phenoxyacetophenone was prepared by refluxing 4-fluoroaceotone and phenol in DMAc for 16 hours. The solvent was removed under reduced pressure and the reside subjected to standard ethyl acetate/water work-up and the resulting material purified by silica gel chromatography.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07772260B2 |
| 出典データセット | uspto-grants-2010_08 |
| ORD ID | ord-2336461666234a08953253d8164eb22e |
| 出典メモ | uspto-grants-2010_08 |