反应详情

4-Phenoxyacetophenone was prepared by refluxing 4-fluoroaceotone and phenol in DMAc for 16 hours. The solvent was removed under reduced pressure and the reside subjected to standard ethyl acetate/water work-up and the resulting material purified by silica gel chromatography.

1. temperatureby refluxing 4-fluoroaceotone
2. customThe solvent was removed under reduced pressure
3. customthe resulting material purified by silica gel chromatography