Nitric Acid → HCID 86628852、化合物

HRID 504081

反応式

HRID 504081 の反応式
[N+:1]([O-:4])([OH:3])=[O:2].[NH2:5][C@H:6]([C:10]([OH:12])=[O:11])[CH2:7][CH2:8][CH3:9].[N+:13]([O-:16])([OH:15])=[O:14].[NH2:17][C@H:18]([C:22]([OH:24])=[O:23])[CH2:19][CH2:20][CH3:21]>O>[N+:1]([O-:4])([OH:3])=[O:2].[N+:13]([O-:16])([OH:15])=[O:14].[NH2:5][C@H:6]([C:10]([OH:12])=[O:11])[CH2:7][CH2:8][CH3:9].[N+:1]([O-:4])([OH:3])=[O:2].[N+:1]([O-:4])([OH:3])=[O:2].[N+:1]([O-:4])([OH:3])=[O:2].[NH2:17][C@H:18]([C:22]([OH:24])=[O:23])[CH2:19][CH2:20][CH3:21]

参加物

6

反応物 3

HCID 944Nitric AcidHCID 65098L-NorvalineHCID 86628854HCID 86628854、化合物

生成物 2

HCID 86628852HCID 86628852、化合物HCID 86628853HCID 86628853、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Applicants have cost-effectively synthesized Norvaline Nitrate by combining nitric acid and Norvaline, mixing with water, and leaving to crystallize. Further nitratization can take place, yielding Norvaline Dinitrate or Norvaline Trinitrate. An alternative implementation comprises substituting Nitrous Acid (HNO2) for Nitric Acid (HNO3), thus yielding Norvaline Nitrite. Norvaline Nitrite has the same effects as Norvaline Nitrate, the only difference being that it requires one less step to yield Nitric Oxide (NO—). Mixed salts may also be used, such as in the non-limiting example of Norvaline Nitrate-Orotate.

後処理

  1. customleaving
  2. customto crystallize

出典と根拠

ORDレコード
ord-0aa88ed6874d4a1d9beca0cf87c536ae
出典データセット
uspto-grants-2010_08
特許番号
US07777074B2

関連ノート

読み込み中…