Chlorotrimethylsilane → (3,5-Dimethylphenyl)trimethylsilane

HRID 5046

反応式

HRID 5046 の反応式
Br[C:2]1[CH:3]=[C:4]([CH3:9])[CH:5]=[C:6]([CH3:8])[CH:7]=1.Cl[Si:11]([CH3:14])([CH3:13])[CH3:12]>>[CH3:12][Si:11]([CH3:14])([CH3:13])[C:2]1[CH:3]=[C:4]([CH3:9])[CH:5]=[C:6]([CH3:8])[CH:7]=1

参加物

3

反応物 2

HCID 6397ChlorotrimethylsilaneHCID 136357Benzene, 1-bromo-3,5-dimethyl-

生成物 1

HCID 2760843(3,5-Dimethylphenyl)trimethylsilane

実験手順

In the same manner as described in preparation 1, 5-bromo-m-xylene was allowed to react with chlorotrimethylsilane, and afforded TSIX. The yield and properties of product are summarized in Table 1.

後処理

  1. customafforded TSIX
  2. customThe yield

出典と根拠

ORDレコード
ord-a6e9045e32c049c09013afb37b5d1d71
出典データセット
uspto-grants-1993_09
特許番号
US05243010

関連ノート

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