Chlorotrimethylsilane → (3,5-Dimethylphenyl)trimethylsilane

反応式

Br[C:2]1[CH:3]=[C:4]([CH3:9])[CH:5]=[C:6]([CH3:8])[CH:7]=1.Cl[Si:11]([CH3:14])([CH3:13])[CH3:12]>>[CH3:12][Si:11]([CH3:14])([CH3:13])[C:2]1[CH:3]=[C:4]([CH3:9])[CH:5]=[C:6]([CH3:8])[CH:7]=1

参加物

反応物 2

HCID 6397Chlorotrimethylsilane

HCID 136357Benzene, 1-bromo-3,5-dimethyl-

生成物 1

HCID 2760843(3,5-Dimethylphenyl)trimethylsilane

実験手順

In the same manner as described in preparation 1, 5-bromo-m-xylene was allowed to react with chlorotrimethylsilane, and afforded TSIX. The yield and properties of product are summarized in Table 1.

後処理

customafforded TSIX
customThe yield

出典と根拠

ORDレコード: ord-a6e9045e32c049c09013afb37b5d1d71
出典データセット: uspto-grants-1993_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05243010

反応ノート

読み込み中…