Methyl iodide → HCID 178503334、化合物
反応式
[CH3:1][I:2].[CH3:3][CH:4]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[NH:7][C:6](=[S:14])[NH:5]1>CC(C)=O>[IH:2].[CH3:3][CH:4]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[N:7]=[C:6]([S:14][CH3:1])[NH:5]1参加物
4
実験手順
Methyl iodide (0.43 ml, 6.94 mmol) was added to a solution of 4-methyl-3,4-dihydro-1H-quinazoline-2-thione (410 mg, 2.30 mmol) in acetone (5 ml). The mixture was stirred for 15 min (r.t.), and the title compound (500 mg, 67%) was isolated from the reaction mixture by filtration.
出典と根拠
- ORDレコード
- ord-15b4bf821c1e4bfdae471fb24b215277
- 出典データセット
- uspto-grants-2010_08
- 特許番号
- US07781441B2
反応ノート
読み込み中…