Aminoacetaldehyde dimethyl acetal → HCID 44997787、化合物
反応式
C([O:3][C:4](=O)[C:5]([NH:7][CH2:8][CH3:9])=[O:6])C.[CH3:11][O:12][CH:13]([O:16][CH3:17])[CH2:14][NH2:15]>CC(O)C>[CH3:11][O:12][CH:13]([O:16][CH3:17])[CH2:14][NH:15][C:4](=[O:3])[C:5]([NH:7][CH2:8][CH3:9])=[O:6]参加物
4
実験手順
59.9 g (412.6 mM) of ethyl(ethylamino)(oxo)acetate and 45 ml (412.6 mM) of (2,2-dimethoxyethyl)amine in 480 ml of 2-propanol were stirred at room temperature for 16 h. A white precipitate was filtered, washed with 2-propanol and dried under vacuum, to give 67.8 g of N-(2,2-dimethoxyethyl)-N′-ethylethanediamide. Yield: 80.5%.
後処理
- filtrationA white precipitate was filtered
- washwashed with 2-propanol
- customdried under vacuum
出典と根拠
- ORDレコード
- ord-906a573158c14fc890fa8e831f12f7bc
- 出典データセット
- uspto-grants-2015_08
- 特許番号
- US09102632B2
反応ノート
読み込み中…