Propane → Bromine

HRID 51295

反応式

HRID 51295 の反応式
[CH3:1][CH2:2][CH3:3].[Br:4][Br:5]>>[Br:4][Br:5].[Br:4][CH:2]([CH3:3])[CH3:1].[Br:4][CH2:1][CH2:2][CH3:3]

参加物

5

反応物 2

HCID 6334PropaneHCID 24408Bromine

生成物 3

HCID 63582-Bromopropane収率 88.9%HCID 78401-Bromopropane収率 11.1%HCID 24408Bromine収率 100%

反応条件

温度
270 °C

実験手順

A mixture of propane (6.0 ml/minute) and bromine (Br2 0.30 ml/hour) was passed into a reactor (glass tube ID 0.38″, heating zone length 4″), which was heated to 270° C. The effluent was analyzed by GC/MS. 100% bromine conversion with 88.9% 2-bromopropane selectivity and 11.1% 1-bromopropane selectivity were obtained.

後処理

  1. customwas passed into a reactor
  2. temperature(glass tube ID 0.38″, heating zone length 4″), which

出典と根拠

ORDレコード
ord-0ef39192c2a34d6fb98eab6abaa9dad6
出典データセット
uspto-grants-2004_03
特許番号
US06713655B2

関連ノート

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