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HRID 517523作成日：2026年10月27日

(S)-3-amino-2-[4-(4-fluorobenzyl)piperazin-1-yl]propanoate trihydrochloride → methyl (S)-3-amino-2-[4-(4-fluorobenzyl)piperazin-1-yl]propanoate trihydrochloride

https://huagongshe.com/reaction/517523

反応式

関与物質

役割名称HCID仕込み量
反応物(S)-3-amino-2-[4-(4-fluorobenzyl)piperazin-1-yl]propanoate trihydrochlorideHCID 68088326—
反応物methyl (S)-3-tert-butoxycarbonylamino-2-(4-ethylpiperazin-1-yl)propanoateHCID 86667916—
生成物methyl (S)-3-amino-2-[4-(4-fluorobenzyl)piperazin-1-yl]propanoate trihydrochlorideHCID 86667914—

反応手順

In a manner similar to example 2-3, starting from 5.3 g (13.4 mmol) of methyl (S)-3-tert-butoxycarbonylamino-2-(4-ethylpiperazin-1-yl)propanoate, 5.4 g (100%) of (S)-3-amino-2-[4-(4-fluorobenzyl)piperazin-1-yl]propanoate trihydrochloride are obtained in the form of a beige solid.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09115102B2
出典データセットuspto-grants-2015_08
ORD IDord-363887cf31a64b979487d6a423891139
出典メモuspto-grants-2015_08