反応式
[CH2:1]([C:4](=[CH:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH:5]=[O:6])[CH2:2][CH3:3]>[Pd].[C]>[CH2:1]([CH:4]([CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH:5]=[O:6])[CH2:2][CH3:3]参加物
3
反応条件
- 温度
- 75 °C
実験手順
An autoclave was charged with 420 g of 2-propyl-2-heptenal and 4 g of a 5% Pd carbon powder (water content: 56%, manufactured by N.E. Chemcat Corporation), and the mixture was stirred at 75° C. for 1.5 hours under a hydrogen pressure of 1.5 MPa. The reaction product was filtered through a membrane filter (PTFE, 0.5 μm) to obtain 416 g of 2-propylheptanal.
後処理
- filtrationThe reaction product was filtered through a membrane
- filtrationfilter (PTFE, 0.5 μm)
出典と根拠
- ORDレコード
- ord-f577967a37614483969cbe2e27e6788d
- 出典データセット
- uspto-grants-2016_05
- 特許番号
- US09328306B2
関連ノート
読み込み中…