Potassium Carbonate → S 20928

HRID 52289

反応式

HRID 52289 の反応式
Cl.[C:2]1([CH2:12][CH2:13][NH2:14])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1.C(=O)([O-])[O-].[K+].[K+].[CH:21]1([C:25](Cl)=[O:26])[CH2:24][CH2:23][CH2:22]1>O.C(Cl)(Cl)Cl>[C:2]1([CH2:12][CH2:13][NH:14][C:25]([CH:21]2[CH2:24][CH2:23][CH2:22]2)=[O:26])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1

参加物

5

反応物 3

HCID 11430Potassium CarbonateHCID 78705Cyclobutanecarbonyl chlorideHCID 123704372-(1-Naphthyl)ethylamine hydrochloride

生成物 1

HCID 127856S 20928

試薬・触媒・溶媒 1

HCID 22418719Chloroform water溶媒

実験手順

0.01 mol of N-[2-(1-naphthyl)ethyl]amine hydrochloride is dissolved in a water/chloroform (40: 60; vol/vol ) mixture, and 0.02 mol of potassium carbonate is then added with magnetic stirring. The reaction mixture is cooled in an ice bath, and 0.01 mol of cyclobutanecarbonyl chloride is then added dropwise with magnetic stirring.

後処理

  1. additionis then added with magnetic stirring
  2. temperatureThe reaction mixture is cooled in an ice bath

出典と根拠

ORDレコード
ord-8e4b4b7fd8854a2684e0c0c78407b175
出典データセット
uspto-grants-1997_04
特許番号
US05616614

関連ノート

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