化工社化工社 化学情報印刷レポート · 研究参考用
Ammonium Chloride → 6-Methoxybenzo[d]thiazole-2-carboximidamide hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonium Chloride | HCID 25517 | — |
| 反応物 | 2-Cyano-6-methoxy benzothiazole | HCID 342109 | — |
| 反応物 | Sodium Methoxide | HCID 10942334 | — |
| 生成物 | 6-Methoxybenzo[d]thiazole-2-carboximidamide hydrochloride | HCID 118107613 | 75% |
反応手順
6-methoxybenzo[d]thiazole-2-carbonitrile (1 g, 5.26 mmol) was reacted with sodium methoxide (0.28 g, 5.26 mmol) and ammonium chloride (0.6 g, 11 mmol) according to the procedure as described in Example 61, Step B to give the title compound as a white solid (0.96 g, 75%). The compound was characterized by the following spectroscopic data:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09340538B2 |
| 出典データセット | uspto-grants-2016_05 |
| ORD ID | ord-a5da7ede6b604060ad6e1da9b0089605 |
| 出典メモ | uspto-grants-2016_05 |