Benzoyl Peroxide → Divinylbenzene-styrene
反応式
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH:9]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=1[CH:17]=[CH2:18])=[CH2:10].C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>C1(C)C=CC=CC=1.CCCCCCCC>[CH:9]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=1[CH:17]=[CH2:18])=[CH2:10].[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1参加物
6
実験手順
It is stirred at room temperature for 30 minutes and then is introduced the monomer system prepared separately consisting of g 100 of styrene, g 67.5 of divinylbenzene (50%) in toluene (225 ml) and n-octane (75 ml) containing 3 g of benzoyl peroxide. The polymerization is carried out by stirring (350 rpm) for 10 hours at 80° C.
後処理
- additionis introduced the monomer system
- customprepared separately
- stirringby stirring (350 rpm) for 10 hours at 80° C.
出典と根拠
- ORDレコード
- ord-445013eb9d6b4372b91d441d2c130c81
- 出典データセット
- uspto-grants-1993_09
- 特許番号
- US05244855
反応ノート
読み込み中…