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Methyl 2-iodo-4-nitrobenzoate → Methyl 2-({3-[(tert-butoxycarbonyl)amino]phenyl}ethynyl)-4-nitrobenzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 2-iodo-4-nitrobenzoate | HCID 232745 | — |
| 反応物 | tert-Butyl 3-ethynylphenylcarbamate | HCID 11275982 | — |
| 生成物 | Methyl 2-({3-[(tert-butoxycarbonyl)amino]phenyl}ethynyl)-4-nitrobenzoate | HCID 57961859 | 87% |
反応手順
This compound was prepared according to the procedure of Example B19 step C, using tert-butyl (3-ethynylphenyl)carbamate and methyl 2-iodo-4-nitrobenzoate as the starting materials in 87% yield. LCMS calculated for C21H21N2O6(M+H)+: m/z=397.1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08871753B2 |
| 出典データセット | uspto-grants-2014_10 |
| ORD ID | ord-6f507852724743249a63560f1d1103b7 |
| 出典メモ | uspto-grants-2014_10 |