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HRID541760

反应详情

EQUATION

反应方程式

HRID 541760 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)c1ccc([N+](=O)[O-])cc1I
HCID232745

methyl 2-iodo-4-nitrobenzoate

C8H6INO4

结构：C#Cc1cccc(NC(=O)OC(C)(C)C)c1
HCID11275982

tert-butyl 3-ethynylphenylcarbamate

C13H15NO2

PRODUCTS

生成物

1
结构：COC(=O)c1ccc([N+](=O)[O-])cc1C#Cc1cccc(NC(=O)OC(C)(C)C)c1
HCID57961859

未命名化合物

收率 87%

PROCEDURE

实验过程

This compound was prepared according to the procedure of Example B19 step C, using tert-butyl (3-ethynylphenyl)carbamate and methyl 2-iodo-4-nitrobenzoate as the starting materials in 87% yield. LCMS calculated for C21H21N2O6(M+H)+: m/z=397.1.

WORKUP

后处理

  1. customThis compound was prepared