化工社化工社 化学情報印刷レポート · 研究参考用
2-Propenoic acid, 3-hydroxypropyl ester → Isopropenylphosphonic Acid Hydroxypropylacrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Propenoic acid, 3-hydroxypropyl ester | HCID 33101 | — |
| 反応物 | Ammonium Persulfate | HCID 62648 | — |
| 反応物 | Peroxydisulfate | HCID 107879 | — |
| 反応物 | Isopropenylphosphonic acid | HCID 557541 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Isopropenylphosphonic Acid Hydroxypropylacrylate | HCID 86739384 | — |
反応手順
Using the apparatus and methodology as described in Example 1, isopropenyl phosphonic acid (61.6 g, 54%, 0.27 mole), hydroxypropylacrylate (16.6 g, 0.13 mole) and water (121.8 g) were charged in the reactor. Ammonium persulfate (6 g) was added. After 11/2 hours of reflux, 6 g additional persulfate was added followed by an equivalent reflux period. The final pH of the yellow solution was 0.72.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04446028 |
| 出典データセット | uspto-grants-1984_05 |
| ORD ID | ord-5d4d50ba7f4644d680f84acc41bdccb2 |
| 出典メモ | uspto-grants-1984_05 |