反应详情

Using the apparatus and methodology as described in Example 1, isopropenyl phosphonic acid (61.6 g, 54%, 0.27 mole), hydroxypropylacrylate (16.6 g, 0.13 mole) and water (121.8 g) were charged in the reactor. Ammonium persulfate (6 g) was added. After 11/2 hours of reflux, 6 g additional persulfate was added followed by an equivalent reflux period. The final pH of the yellow solution was 0.72.

1. additionwere charged in the reactor
2. temperatureAfter 11/2 hours of reflux
3. temperaturean equivalent reflux period