1-Propanamine, acetate → HCID 178456849、化合物

HRID 543661

反応式

HRID 543661 の反応式
CS[C:3]1[N:8]=[C:7]([OH:9])[C:6]([C:10]([O:12][CH2:13][CH3:14])=[O:11])=[CH:5][N:4]=1.C(O)(=O)C.[CH2:19]([NH2:22])[CH2:20][CH3:21]>O>[CH2:19]([NH:22][C:3]1[N:8]=[C:7]([OH:9])[C:6]([C:10]([O:12][CH2:13][CH3:14])=[O:11])=[CH:5][N:4]=1)[CH2:20][CH3:21]

参加物

4

反応物 2

HCID 122036631-Propanamine, acetateHCID 178418871HCID 178418871、化合物

生成物 1

HCID 178456849HCID 178456849、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

2-Methylthio-5-ethoxycarbonyl-4-hydroxypyrimidine (2 mmol, 428 mg) was heated on an oil bath at 160° C. with n-propylamine acetate (1 ml) for 1 hour. The semi solid was cooled and then treated with 50 ml boiling water, and the solid product was filtered off (yield 400 mg, 88%)

後処理

  1. temperatureThe semi solid was cooled
  2. additiontreated with 50 ml
  3. filtrationthe solid product was filtered off (yield 400 mg, 88%)

出典と根拠

ORDレコード
ord-29a8e092abdd40efa21bc881d67aaf27
出典データセット
uspto-grants-1984_05
特許番号
US04447422

関連ノート

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