化工社化工社 化学情報印刷レポート · 研究参考用
1-Propanamine, acetate → HCID 178456849、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Propanamine, acetate | HCID 12203663 | — |
| 反応物 | HCID 178418871 | HCID 178418871 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178456849 | HCID 178456849 | — |
反応手順
2-Methylthio-5-ethoxycarbonyl-4-hydroxypyrimidine (2 mmol, 428 mg) was heated on an oil bath at 160° C. with n-propylamine acetate (1 ml) for 1 hour. The semi solid was cooled and then treated with 50 ml boiling water, and the solid product was filtered off (yield 400 mg, 88%)
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04447422 |
| 出典データセット | uspto-grants-1984_05 |
| ORD ID | ord-29a8e092abdd40efa21bc881d67aaf27 |
| 出典メモ | uspto-grants-1984_05 |