Propylamine → HCID 53782809、化合物
反応式
[C:1]([NH:3][C:4]1[CH:9]=[CH:8][N:7]=[C:6]([S:10][CH3:11])[N:5]=1)#[N:2].[CH2:12]([NH2:15])[CH2:13][CH3:14]>C(#N)C>[CH2:12]([N:15]=[C:1]([NH2:2])[NH:3][C:4]1[CH:9]=[CH:8][N:7]=[C:6]([S:10][CH3:11])[N:5]=1)[CH2:13][CH3:14]参加物
4
実験手順
A mixture of 4-cyanoamino-2-methylthiopyrimidine (0.83 g.) and n-propylamine (0.6 ml.) was heated under reflux in acetonitrile (20 ml.) for 1 hour. The solvent was evaporated in vacuo and the residue suspended in dilute aqueous sodium hydroxide. The solid was collected, washed with water and dried to give 4-(2-propylguanidino)-2-methylthiopyrimidine, m.p. 177°-178°.
後処理
- temperaturewas heated
- customThe solvent was evaporated in vacuo
- customThe solid was collected
- washwashed with water
- customdried
出典と根拠
- ORDレコード
- ord-c91a9f7f7ff34155bef03e449cc34e15
- 出典データセット
- uspto-grants-1984_05
- 特許番号
- US04451463
反応ノート
読み込み中…