化工社化工社 化学情報印刷レポート · 研究参考用
4-Fluorothiophenol → Ethanethioic acid trans-(+/-)-S-[5-[[(4-fluorophenyl)thio]methyl]tetrahydro-3-furanyl]ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Fluorothiophenol | HCID 67789 | — |
| 反応物 | Diisopropylethylamine | HCID 81531 | — |
| 反応物 | Ethanethioic acid trans(+/-)-S-[tetrahydro-5-[[[(trifluoromethyl)sulfonyl]oxy]methyl]-3-furanyl]ester | HCID 86750748 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Ethanethioic acid trans-(+/-)-S-[5-[[(4-fluorophenyl)thio]methyl]tetrahydro-3-furanyl]ester | HCID 86750751 | — |
反応手順
The title compound is prepared by the procedure of Example 23 using 0.308 g of product from Example 22 in 1 ml of methylene chloride, 107 microliter of 4-fluorothiophenol, and 174 microliter of Hunig's base to give 0.236 g of the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05623081 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-1f1cec4eec9c44a0b79c59d2ea655bfc |
| 出典メモ | uspto-grants-1997_04 |