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HRID54774

反应详情

EQUATION

反应方程式

HRID 54774 的结构方程式

REACTANTS

反应物

3
结构：Fc1ccc(S)cc1
HCID67789

4-Fluorothiophenol

C6H5FS

结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：CC(=O)S[C@@H]1CO[C@@H](COS(=O)(=O)C(F)(F)F)C1
HCID86750748

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)S[C@@H]1CO[C@@H](CSc2ccc(F)cc2)C1
HCID86750751

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

The title compound is prepared by the procedure of Example 23 using 0.308 g of product from Example 22 in 1 ml of methylene chloride, 107 microliter of 4-fluorothiophenol, and 174 microliter of Hunig's base to give 0.236 g of the desired product.