TIBA isododecane → 2,3,5-Triiodobenzoic acid
反応式
[CH:1]1[C:6]([I:7])=[C:5]([I:8])[C:4]([C:9]([OH:11])=[O:10])=[CH:3][C:2]=1[I:12].CCCCCCCCCC(C)C>C1(C)C=CC=CC=1>[CH:1]1[C:6]([I:7])=[C:5]([I:8])[C:4]([C:9]([OH:11])=[O:10])=[CH:3][C:2]=1[I:12]参加物
3
実験手順
33.3 ml of TIBA/isododecane solution (101 g/L) was mixed with 7.9 cc of MAO/toluene solution (Albemarle −30% wt) to obtain a MAO/TIBA molar ratio of 2:1. The solution was stirred for 1 hour at room temperature. Then, 69 mg of A-1 was dissolved in the solution.
出典と根拠
- ORDレコード
- ord-7c8ef107c3634e86a66b5e20aa7b8cba
- 出典データセット
- uspto-grants-2011_05
- 特許番号
- US07943716B2
反応ノート
読み込み中…