Acrylic Acid → 2-Propenoic acid, aluminum salt (3:1)
反応式
C([O-])(C)C.C([O-])(C)C.C([O-])(C)C.[Al+3:13].[C:14]([OH:18])(=[O:17])[CH:15]=[CH2:16]>>[C:14]([O-:18])(=[O:17])[CH:15]=[CH2:16].[C:14]([O-:18])(=[O:17])[CH:15]=[CH2:16].[C:14]([O-:18])(=[O:17])[CH:15]=[CH2:16].[Al+3:13]参加物
3
反応条件
- 温度
- 32 °C
実験手順
Into the flask described hereinabove there were placed 204.2 grams of aluminium tri-isopropanolate to which 216 grams of acrylic acid were added during 8 minutes at room temperature (25° C.). The procedure was as set forth hereinabove. Owing to the reaction heat, the temperature increased to 32° C. The resultant product was a white, solid substance. The rotary evaporator heating then was switched on and gradually heated to 70° C. At the same time the vacuum was gradually adjusted to 24 mbar. The isopropanol was thereby expelled yielding a white powder.
後処理
- additionwere added during 8 minutes at room temperature (25° C.)
- temperature