Hydrazine hydrate (1:1) → 2,2-Dimethyl-4-pentenohydrazide
反応式
[CH3:1][C:2]([CH3:10])([CH2:7][CH:8]=[CH2:9])[C:3](OC)=[O:4].O.[NH2:12][NH2:13]>CO>[CH3:1][C:2]([CH3:10])([CH2:7][CH:8]=[CH2:9])[C:3]([NH:12][NH2:13])=[O:4]参加物
4
反応条件
- 温度
- 60 °C
実験手順
To a solution of methyl 2,2-dimethyl-4-pentenoate (1 g) in MeOH (2 ml) was added hydrazine monohydrate (2.7 ml). The solution was heated in a close microwave vial at 60° C. for 12 h. Volatiles were evaporated in vacuo to give 1 g of the title compound as a yellow pale foam, which was used without further purification.
後処理
- customVolatiles were evaporated in vacuo
出典と根拠
- ORDレコード
- ord-6389608f00bc4024aa9b779acd323f32
- 出典データセット
- uspto-grants-2011_05
- 特許番号
- US07947683B2
反応ノート
読み込み中…